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This paper was presented to the 1992 National Conference of Standards Laboratories in Washington, DC and is © Copyright 1992 by Alternate Systems, Plano, Texas. (800) 928-XRAY. All rights reserved. If you need to use parts or all of this paper, please contact us for permission. Thanks. You can find the original of this paper in the Proceedings of this conference.

NON-DESTRUCTIVE MEASUREMENT OF COATINGS
ON ELECTRONIC PACKAGES

Peter W. Wright
CEO
Alternate Systems
2333 Claridge Circle
Plano, Texas 75075
972-964-3124
FAX 972-423-5464

Abstract
The ability to measure conductive coatings applied to electronic packages has improved significantly. Beta Backscatter replaced microscopic cross-sectioning in most applications because of it's ability to resolve thinner coatings than possible with micro-sectioning. In the last ten years, x-ray fluorescence (XRF) coating measurement systems have replaced beta backscatter systems because of XRF's lower random error and because of it's abilities for material discrimination and measurement of several layers on very small areas. While the ability to measure coatings has improved, the potential sources of error have changed. It is interesting that an XRF instrument may produce acceptable results on it's calibration standards and not produce accurate results on the samples being measured. This paper will discuss the sources of error involved with measurement of coatings on electronic packages and present methods for eliminating their effects on measurement.

Scope
This paper will cover the measurement of gold, nickel, and tin-lead solder on copper, phosphor bronze, kovar (glass sealing alloys), and printed circuit board substrates. It will begin with a discussion of accuracy and precision, and end with a measurement assurance procedure. Specific adjustment procedures should be found in the appropriate instrument instruction manual.

Abstract
Accuracy and Precision

Principle of Measurement
Gold and Nickel Measurements on Copper
Gold and Nickel Measurements on Phosphor Bronze
Gold and Nickel Measurements on Kovar and Other Glass-Sealing Alloys
Gold and Nickel Measurements on FR-4 Circuit Board Substrates
Tin-Lead Solder on Copper, FR-4 Circuit Board Substrates, and Kovar
Tin-Lead Solder on Phosphor Bronze
Adjustments for Part Geometry
Measurement Assurance
Conclusion

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Alternate Systems
2333 Claridge Circle
Plano, TX 75075 USA

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